| 第 31 卷第 5 期 |  | Vol. 31 No. 5 | | 2001 年 10 月 | Oct 2001 |
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所屬欄目：分析與測試
1-(2-氯苯基)-5(4H)-四唑啉酮氣相色譜法的分析研究 |
| 潘忠穩; 姚瓊; 凌冰(安徽省化工研究院) |
| 摘 要：用 5 %OV - 17,長(cháng)度為 2m的玻璃填充柱 ,以硝基苯為內標物 ,在 140℃柱溫下 ,用FID檢測器對 1 (2 氯苯基 ) 5 (4H ) 四唑啉酮進(jìn)行定量分析。該方法變異系數為0 2 2 % ,平均回收率 99 8% ,線(xiàn)性相關(guān)系數為 0 99998 |
| 關(guān)鍵詞：氣相色譜法; 1（2氯苯基）5（4H）四唑啉酮; 分析 |
| 中圖分類(lèi)號：TQ252.8 文獻標識碼：A 文章編號：1009-9212(2001)05-0047-02 |
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| Analysis of 1-(2-Chlorophenyl)-5(4H)-tetrazolinone by Gas Chomatography |
| PAN Zhong wen; YAO Qiong; LING Bing （Anhui Research Institute of Chemical Industry; Hefei 230041） |
| Abstract：chlorophenyl) 5(4H) tetrazolinone was analyzed by gas chomatography with flame ionization detection on Φ2.5mm×2m 5% OV-17/Gas chromosorb W HP (0.147～0.175mm) packed column. The column temperature was 140℃. The ionization temperature was 240℃ and the detection temperature was 240℃. The linear relationship of this method was very good. The standard deviated and viation coefficient were 0.21% and 0.22% respectively. |
| Key words：chlorophenyl） 5（4H） tetrazolinone; analysis; gas chomatography |
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收稿日期：2001-08-12
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