| 第 32 卷第 1 期 |  | Vol. 32 No. 1 | | 2002 年 2 月 | Feb 2002 |
|
所屬欄目：其它
AlCl_3/D_(72)樹(shù)脂催化合成水楊酸甲酯的研究 |
| 鄧宇(天津輕工業(yè)學(xué)院化工系) |
| 摘 要：用AlCl3/D72 作催化劑 ,合成水楊酸甲酯研究了催化劑用量、反應時(shí)間、反應溫度、醇酸比對反應的影響 ,確定了反應優(yōu)惠條件、催化劑用量為 1% (與原料水楊酸的質(zhì)量比 )、反應時(shí)間 3h、反應溫度 65～ 70℃、醇酸比 3～ 4∶1(mol/mol不加帶水劑 )或 1.5～ 2∶1(mol/mol加帶水劑 ) ,收率大于 92 % |
| 關(guān)鍵詞：催化劑; 合成; 水楊酸甲酯 |
| 中圖分類(lèi)號：O625.21 文獻標識碼：A 文章編號：1009-9212(2002)01-0034-01 |
|
| Study on Synthesis of Methyl Salicylate by AlCl_3/D_(72) Resin. |
| DENG Yu.（Department of Chemical Engineering; Tianjin University of Light Industry; Tianjin 300222） |
| Abstract：The synthesis of methyl salicylate, AlCl 3/D 72 Resin as catalyst,the influences of Catalyst dosage, reaction time, reaction temperature and the ratio of alcohol to acid on synthetising methyl salicylate were studied. The experiment results showed that the optimum condition was as follows: the quality proportion of salicylic acid and catalyst dosage 100∶1, reaction time 3h, reaction temperature 65～70℃, the ratio of alcohol to acid 3～4∶1 (not carrying water reagent) or 1.5～2∶1 (with carring water reage... |
| Key words：catalyst; systhesis; methyl salicylate |
|
收稿日期：2001-10-08
|
| 閱讀全文 |
|