| 第 32 卷第 2 期 |  | Vol. 32 No. 2 | | 2002 年 4 月 | Apr 2002 |
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所屬欄目：其它
氨基磺酸催化合成氯乙酸異戊酯 |
| 楊春霞; 付興華; 劉思全(濟南大學(xué)化工學(xué)院; 山東濟南) |
| 摘 要：采用氨基磺酸作催化劑 ,合成氯乙酸異酯。反應最佳條件為 :異戊醇∶氯乙酸 (摩爾比 )為 1∶1.3,在 100～110℃反應 2h ,氯乙酸異戊酯的收率為 91.4 % |
| 關(guān)鍵詞：氯乙酸異戊酯; 催化劑; 合成 |
| 中圖分類(lèi)號：TQ225.5 文獻標識碼：A 文章編號：1009-9212(2002)02-0024-01 |
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| Synthesis of Chloroacetic Acid Isoamyl Ester With Aminosulfonic Acid as Catalyst |
| Yang Chun xia; et al（School of Chemical Engneering; Jinan University; Jinan 250022; China） |
| Abstract：Chloroacetic acid isoamyl ester was synthesized with aminosulfonic acid as catalyst from chloroacetic acid and isoamyl alcohol.The optimum operation was that the ratior of isoamyl alcohol and chloroacetic acid was 1∶1.3(mole rate),the reaction temperature about 100～110℃,and time 2h.The yield of the ester was 91.4%. |
| Key words：chloroacetic acid isoamyl ester; catalyst; synthesis |
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收稿日期：2001-12-11
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