| 第 47 卷第 1 期 |  | Vol. 47 No. 1 | | 2017 年 2 月 | Feb 2017 |
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所屬欄目：分析與測試
電感耦合等離子體發(fā)射光譜法（ICP-AES）測定鹽湖鹵水及鹽業(yè)制品中的硫、硼 |
| 鄒 娟，楊 清，羅 穩，劉雨星，楊三妹，謝 超*
（化工部長(cháng)沙設計研究院 湖南省鉀及伴生物工程技術(shù)研究中心，湖南 長(cháng)沙 410116） |
| 摘 要：建立了一種采用電感耦合等離子體原子發(fā)射光譜儀（ICP-AES）測定鹽湖鹵水及鹽業(yè)制品中硫、硼的方法。樣品經(jīng)過(guò)簡(jiǎn)單稀釋后即可測試，元素檢出限為0.04～0.38 mg／L，加標回收率為97.56%～102.4%，相對標準偏差RSD<3.5%，方法簡(jiǎn)單快捷，精密度好，準確度高，適用于鹽湖鹵水及鹽業(yè)制品中硫、硼的測定。 |
| 關(guān)鍵詞：電感耦合等離子體；鹽湖鹵水；鹽業(yè)制品；硫；硼 |
| 中圖分類(lèi)號：O657 文獻標識碼：A 文章編號：1009-9212（2017）01-0063-03 |
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| Determination of Sulfur and Boron in Salt Lake Brine and Salt Products Using Inductively Coupled Plasma Atomic Emission Spectrometry |
| ZOU Juan, YANG Qing, LUO Wen, LIU Yu-xing, YANG San-mei, XIE Chao*
(Changsha Design & Research Institute, the Ministry of Chemical Industry, Hunan Engineering Research Center of Potassium and its Co-existed Resources, Changsha 410116, China) |
| Abstract：A method was developed to determine sulfur and boron in salt Lake brine and salt products using inductively coupled plasma atomic emission spectrometry (ICP-AES). The samples were determined after simply diluting with water. The detection-limitation of element was 0.04～0.38 mg/L; the recovery was between 97.56% and 102.4%; and the relative standard deviation was less than 3.5%. This method was simply and rapid with great precision and high accuracy, which could be used to analyze S and B in salt Lake brine and salt products. |
| Key words：ICP-AES; salt lake brine; salt products; sulfur; boron |
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作者簡(jiǎn)介：鄒 娟（1982-），女，湖南邵陽(yáng)人，研究方向：分析化學(xué)（E-mail: 258157149@qq.com）。
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聯(lián) 系 人：謝 超，高級工程師，研究方向：鹽湖化工工藝。
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收稿日期：2017-01-05
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