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第 33 卷第 2 期Vol. 33 No. 2
2003 年 4 月Apr 2003

所屬欄目:其它

環(huán)已二醇二丙烯酸酯的合成工藝
蔣衛和; 鄧劍如; 屈鎧甲(湖南大學(xué)化學(xué)化工學(xué)院; 岳陽(yáng)昌德化工實(shí)業(yè)有限公司; 湖南長(cháng)沙; 410082; 湖南岳陽(yáng); 414003)
摘 要:用濃硫酸作催化劑 ,環(huán)已烷作帶水劑 ,對甲氧基苯酚作阻聚劑 ,利用直接酯化法合成環(huán)已二醇二丙烯酸酯 ,同時(shí)就助劑作用和用量對反應影響進(jìn)行探討 ,確定了合適的合成工藝路線(xiàn)。
關(guān)鍵詞:環(huán)已二醇二丙烯酸酯; 直接酯化; 合成工藝
中圖分類(lèi)號:TQ225.24  文獻標識碼:A  文章編號:1009-9212(2003)02-0038-02
The Synthetic Process of Cyclohexandiol Propane Diacrylate
JIANG Wei-he etc.(Chemistry and Chemical Engineering College; Hunan University; Changsha Hunan; 410082; China)
Abstract:Cyclohexandiol propane diacrylate was obtained by the direct esterifying method with sulphuric acid as Catalyst, cyclohexane as dehydrant, and p-metheroxyl phenol as retarded. The influences of function and the content of promoter initially was discussed. A suitable synthetic technology route was given.
Key words:cyclohexandiol propane diacrylate; direct esterifying; dynamics; technology route
收稿日期:2002-12-05
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