| 第 33 卷第 3 期 |  | Vol. 33 No. 3 | | 2003 年 6 月 | Jun 2003 |
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所屬欄目：其它
雜多酸(鹽)催化新型香料草莓酯的合成 |
| 劉杰鳳; 農蘭平; 蔣維(茂名學(xué)院; 廣東茂名; 525000) |
| 摘 要：采用硅鎢酸鋁作催化劑 ,以乙酰乙酸乙酯和 1 ,2 丙二醇為原料合成草莓酯。優(yōu)化的反應條件為 :0 2mol乙酰乙酸乙酯 ,0 2mol1 ,2 丙二醇 ,40ml環(huán)己烷 ,0 3 g硅鎢酸鋁 ,反應 3 5h ,草莓酯收率達 81 6%。產(chǎn)物經(jīng)理化檢驗和紅外光譜確證 |
| 關(guān)鍵詞：草莓酯; 雜多酸; 合成 |
| 中圖分類(lèi)號：TQ655 文獻標識碼：A 文章編號：1009-9212(2003)03-0019-02 |
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| Synthesis of a New Type Perfume fraistone Catalyzed by Heteropoly Acids(salt) |
| LIU Jie feng etc.（Maoming college; Guangdong maoming 525000; China） |
| Abstract：Fraistone was synthesized with reaction of Ehyl Acetyl acetate and 1,2 Propanediol, by aluminnm silicolungstie as catatlyst. The optimum conditions are follows: the ratio of ethyl acetate, 1,2 Propanediol, Cyclohexane,Aluminnm Silicolungstie is 0.2?mol:0.2?mol:40?ml:0.3?g, reaction for 3.5 hours.The yield reaches 81.6%. The product was characterized by the physical and chemical character, and spectra. |
| Key words：fraistone; heteropoly acids; synthesis |
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收稿日期：2003-04-03
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