第 33 卷第 6 期 |  | Vol. 33 No. 6 | 2003 年 12 月 | Dec 2003 |
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所屬欄目:分析與測試
HPLC法測定吡·咪懸浮種衣劑中的有效成分 |
金晨鐘; 劉桂英; 胡利瓊(湖南省婁底農科所; 南京師范大學(xué)鎮江實(shí)驗中學(xué); 湖南婁底; 江蘇鎮江) |
摘 要:介紹了用一根C18柱,在同一色譜條件下,以甲醇和水為流動(dòng)相,對吡蟲(chóng)啉和咪鮮胺混配制劑進(jìn)行定量分析。該方法的標準偏差分別為0.012和0.014,變異系數分別為1.07%和2.64%,線(xiàn)性相關(guān)系數分別為0.9996和0.9997,回收率分別為98.93%~102.79%和98.7%~100.49%。 |
關(guān)鍵詞:吡蟲(chóng)啉; 咪鮮胺; 反相高效液相色譜 |
中圖分類(lèi)號:TQ455.4+7 文獻標識碼:A 文章編號:1009-9212(2003)06-0059-02 |
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Determination of Imidacloprid and Prochloraz for Seed Coating Formulation by HPLC |
JIN Chen zhong; etc (Loudi Research Institute of Agricultural Sciences; Hunan Province; Loudi Hunan 417000; China) |
Abstract:A quantitative analytical method was introduced for seed coating formulation of imidacloprid and prochloraz by reversed phase HPLC with C 18 column and UV?235?nm, methanol and water=60+40(V/V) as mobile phase. The result shows that the standard deviations are 0.012 and 0.014; the coeffients of variation are 1.07% and 2.64%; the linear correlations are 0 9996 and 0 9997; the recoveries are 98 93% 102.79% and 98.75% 100.49%. |
Key words:imidacloprid; prochloraz; HPLC |
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收稿日期:2003-08-17
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