| 第 33 卷第 6 期 |  | Vol. 33 No. 6 | | 2003 年 12 月 | Dec 2003 |
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所屬欄目：其它
6-硝基胡椒基酸合成新方法 |
| 楊廣照; 申?yáng)|升; 劉小帆(湘潭大學(xué)化學(xué)學(xué)院; 湖南湘潭) |
| 摘 要：報道了直接以黃樟油為原料,經(jīng)硝化和氧化制備6 硝基胡椒基酸的新工藝。采用調整反應溫度和硝酸濃度等因素對硝化反應進(jìn)行了探討;采用正交實(shí)驗優(yōu)化了氧化反應參數,獲得了較好的工藝條件。 |
| 關(guān)鍵詞：6-硝基胡椒基酸; 黃樟油; 硝化反應; 氧化反應 |
| 中圖分類(lèi)號：TQ245 文獻標識碼：A 文章編號：1009-9212(2003)06-0025-02 |
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| A New Synthesic Method of 6-Nitro-1,3-Benzodioxide Acid |
| YANG Guang zhao; etc（College of Chemistry; Xiangtan University; Xiangtan Hunan 411105; China） |
| Abstract：A new method including the nitration and oxidation of synthesis of 6 Nitro 1,3 benzodioxide acid was introduced. The raw material is safrole. In the process of nitration, the synthesis temperature and the nitric acid concentration was tested. The optimum conditions of oxidation were studied by the way of orthogonal experimental design. |
| Key words：Nitro-1; 3-benzodioxide acid; Safrole; nitration; oxidation |
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收稿日期：2003-05-09
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