第 31 卷第 2 期 |  | Vol. 31 No. 2 | 2001 年 4 月 | Apr 2001 |
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所屬欄目:其它
改性環(huán)糊精手性毛細管柱的研制及拆分機理 |
閻建輝; 唐闊文;(岳陽(yáng)師范學(xué)院化學(xué)化工系;) |
摘 要:合成了四種改性 β 環(huán)糊精手性固定相 ,對幾類(lèi)手性化合物和芳香異構體進(jìn)行了拆分 ,并研究了其可能的拆分機理 ,同時(shí)對毛細管柱的色譜性能進(jìn)行了考察。 |
關(guān)鍵詞:改性環(huán)糊精; 手性固定相; 毛細管氣相色譜; 拆分機理; |
中圖分類(lèi)號:O657.8 文獻標識碼:A 文章編號:1009-9212(2001)02-0013-03 |
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Preparation of Derivatized Cyclodextrins Capillary columns and Investigation on Separation Mechanism |
YAN Jian hui; TANG Kuo wen (College Chemical Engineering; Yueyang Normal University; Hunan Yueyang 414000; China); |
Abstract:Four derivatized cyclodextrins have been synthesized and coated in fused silica capillary columns as stationary phases. A series of enantiomers have been separated on the four stationary phases. The separation mechanism of them has been studied, and the chromatography performance has been investigated. |
Key words:derivatized cyclodextrins; chiral stationary phases; capillary gas chromatography; separation mechanism; |
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收稿日期:2000-12-25
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