| 第 35 卷第 3 期 |  | Vol. 35 No. 3 | | 2005 年 6 月 | Jun 2005 |
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所屬欄目：其它
α,α-二苯基-4-哌啶甲醇催化氫化合成工藝研究 |
| 蔣崇文; 何德文(中南大學(xué)化學(xué)化工學(xué)院; 湖南長(cháng)沙) |
| 摘 要：研究了催化氫化法合成α,α-二苯基-4-哌啶甲醇的工藝。以Pt/C為催化劑,考察了反應溶劑,壓力,反應時(shí)間和催化劑添加比例對催化加氫反應的影響。在優(yōu)惠的工藝條件下,α,α-二苯基-4-哌啶甲醇的收率可達92.4%,產(chǎn)品純度為98.8%。 |
| 關(guān)鍵詞：催化加氫; α; α-二苯基-4-哌啶甲醇; 合成 |
| 中圖分類(lèi)號：TQ46 文獻標識碼：A 文章編號：1009-9212(2005)03-0022-02 |
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| Synthesis of α,α-diphenyl-4-piperidinomethanol by catalytic Hydrogenation |
| JIANG Chong-wen; He De-wen（School of Chemistry and Chemical Engineering of Central South University; Changsha 410083; China） |
| Abstract：A novel technology of hydrogenation for synthesizing the α, α-diphenyl-4-piperidinomethanol was proposed by using Pt/C catalyst. The effects of solvents, pressure, temperature, catalyst amount and reaction time on the yield were investigated. Under the optimum reaction condition, the result showed that the yield can reach 92.4% and the purity was up to 98.8%. |
| Key words：catalytic hydrogenation; α; α-diphenyl-4-piperidinomethanol; synthesis |
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收稿日期：2005-01-05
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