| 第 35 卷第 6 期 |  | Vol. 35 No. 6 | | 2005 年 12 月 | Dec 2005 |
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所屬欄目：農藥及中間體
粉唑醇GC和HPLC分析方法 |
| 魏光; 慕衛; 楊連來(lái); 潘金菊; 劉彥良(山東農業(yè)大學(xué)植物保護學(xué)院; 山東泰安) |
| 摘 要：采用氣相色譜法和液相色譜法分別對粉唑醇進(jìn)行了定性和定量分析。氣相色譜法中以正二十烷為內標物,色譜柱采用3%OV-101 chromosorb AW DMCS 150-177μm1m×3mm玻璃柱,柱溫為195℃,汽化溫和檢測溫均為230℃,方法回收率為99.2%～100.9%,變異系數為0.262%。高效液相色譜法中Nova-PaK C18 250 mm×4.6mm色譜柱,以v(甲醇)+v(水)=851∶5為流動(dòng)相,檢測波長(cháng)為262nm。方法回收率為98.9%～99.4%,變異系數為0.505% |
| 關(guān)鍵詞：粉唑醇; 分析; GC; HPLC |
| 中圖分類(lèi)號：O657.7+1 文獻標識碼：A 文章編號：1009-9212(2005)06-0039-02 |
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| Study on the quantitative analysis method for flutriafol by GC and HPLC |
| WEI Guang; MU Wei; YANG Lian-lai; PAN Jin-ju; LIU Yan-liang（College of Plant Protection; Shandong Agricultural University; Tai'an; Tai'an 271018; China） |
| Abstract：The quantitative analysis method for flutriafol by GC and HPLC was studied.In the gas chromatographic method a 3%OV-101 on Chromosorb AW DMCS 150～177 μ m,1m×3mm(i.d.),glass column was used at column temperature of 195 ℃ and detector temperature of 230℃.The internal standard was n-eicosane.This method had a recovery of 99.2%～100.9%,the coefficient of variation was 0.262%.The operating conditions of high phase liquid chromatographic method were C18 column(250 mm×4.6 mm),v(methanol)∶v(water)=85∶15 as mobile ph... |
| Key words：flutriafol; quantitative analysis; GC; HPLC |
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收稿日期：2005-05-14
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